A new (R) - phenylglycinol hydrochloride, its chemical formula is as follows: the synthesis methods of the compound is in accordance with the molar ratio of 1:5.2:3.0 2-hydroxybenzonitrile, (R) - phenylglycinol respectively with three or three rubidium chloride and samarium chloride in chlorobenzene solution refluxing for 3 days, with oil ether / dichloromethane (volume ratio 7/3) with saturated solution of natural volatile, the target product (R) - phenylglycinol hydrochloride.
【技术实现步骤摘要】
【技术保护点】
一种手性（R）?苯甘氨醇盐酸盐的合成方法，包括合成和分离，所述的合成按照摩尔比为1:5.2:3.0的邻羟基苯甲腈、（R）?苯甘氨醇分别与三氯化铷或与三氯化钐在氯苯溶液中回流反应3天，用石油醚/二氯甲烷（体积比为7/3）配制饱和溶液，自然挥发后，得目标产物（R）?苯甘氨醇盐酸盐。
【技术特征摘要】
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